Microstructural Characterization of Porous Clay-Based Ceramic Composites

Characterization of 3D interconnected microstructural network in mixed ionic and electronic conducting ceramic composites.

The microstructure and connectivity of the ionic and electronic conductive phases in composite ceramic membranes are directly related to device performance. Transmission electron microscopy (TEM) including chemical mapping combined with X-ray nanotomography (XNT) have been used to characterize the composition and 3-D microstructure of a MIEC composite model system consisting of a Ce0.8Gd0.2O2 (...

Synthesis and Characterization of Porous Clay Heterostructures

Porous clay heterostructures (PCH) based on modified montmorillonite were synthesized using different reaction conditions (different hydration degrees, pH values and reaction times). The PCH precursors and PCH were characterized using FTIR Spectroscopy and X-Ray Diffractions (XRD). The XRD results showed that basal distance of porous clay heterostructures was significantly influenced by the mod...

Phase and Microstructural Correlation of Spark Plasma Sintered HfB2-ZrB2 Based Ultra-High Temperature Ceramic Composites

Abstract: The refractory diborides (HfB2 and ZrB2) are considered as promising ultra-high temperature ceramic (UHTCs) where low damage tolerance limits their application for the thermal protection system in re-entry vehicles. In this regard, SiC and CNT have been synergistically added as the sintering aids and toughening agents in the spark plasma sintered (SPS) HfB2-ZrB2 system. Herein, a nove...

Porous Ceramic - Metal Composites Obtained by Infiltration Methods

A. Boczkowska, P. Chabera, Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw, Poland A. J. Dolata, M. Dyzia, Silesian University of Technology, Faculty of Materials Science and Metallurgy, Katowice, Poland A. Oziębło, Institute of Ceramics and Construction Materials, Katowice, Poland A pressure-vacuum infi ltration (T = 720 oC, p = 15 MPa, t = 15 min) and gas...

Microstructural and Mineralogical Characterization of Clay Stabilized Using Calcium-Based Stabilizers